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Senthilkumar, G.
- Mineral Analysis of Coastal Sediment Samples of Tuna, Gujarat, India
Abstract Views :745 |
PDF Views:169
Authors
Affiliations
1 PG & Research Dept. of Physics, Govt. Arts College, Tiruvanamalai-606601, TN, IN
2 Dept. of Physics, University College of Engg., Arani-632317, TN, IN
3 Dept. of Physics, St.Joseph’s College of Engg., Chennai-119, TN, IN
4 Department of Physics, Sacred Heart College, Thirupattur-635601, TN, IN
5 National Institute of Ocean Technology, Pallikaranai, Chennai -601302,TN, IN
1 PG & Research Dept. of Physics, Govt. Arts College, Tiruvanamalai-606601, TN, IN
2 Dept. of Physics, University College of Engg., Arani-632317, TN, IN
3 Dept. of Physics, St.Joseph’s College of Engg., Chennai-119, TN, IN
4 Department of Physics, Sacred Heart College, Thirupattur-635601, TN, IN
5 National Institute of Ocean Technology, Pallikaranai, Chennai -601302,TN, IN
Source
Indian Journal of Science and Technology, Vol 3, No 7 (2010), Pagination: 775-781Abstract
Qualitative analysis was carried out to determine the major and minor constituent minerals present in sediment samples collected at the coastal area of Tuna, Gujarat by FT-IR and XRD technique. From the IR absorption band or the locations of the different peaks, the minerals were identified with the available literature. In addition to the band positions, the sharpness or diffuseness of bands was helpful in the identification of mineral components. The IR study on sediment samples was highly useful in identifying the various minerals in sediments. Further, the representative sediment samples were analyzed by XRD technique to yield more information about the minerals. Both of these methods were non-destructive and can be used in the identification of mineralogical composition. These results confirmed that the applied techniques are relatively quicker and more reliable in mineral analysis.Keywords
Sediment Samples, Mineral Analysis, FT-IR, XRD TechniqueFull Text
References
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- Analysis of Ancient Potteries of Tamilnadu, India by Spectroscopic Techniques
Abstract Views :442 |
PDF Views:127
Authors
Affiliations
1 Post Graduate & Research Dept. of Physics, Government Arts College, Tiruvanamalai-606601, TN, IN
2 Department of Physics, St.Joseph’s College of Engineering, Chennai-119, Tamilnadu, IN
3 Department of Physics, Sacred Heart College, Thirupattur-635601, Tamilnadu, IN
4 Department of Physics, University College of Engineering, Arani-632317, Tamilnadu, IN
5 Anthropology Section, Government Museum, Egmore, Chennai-600008,Tamilnadu, IN
1 Post Graduate & Research Dept. of Physics, Government Arts College, Tiruvanamalai-606601, TN, IN
2 Department of Physics, St.Joseph’s College of Engineering, Chennai-119, Tamilnadu, IN
3 Department of Physics, Sacred Heart College, Thirupattur-635601, Tamilnadu, IN
4 Department of Physics, University College of Engineering, Arani-632317, Tamilnadu, IN
5 Anthropology Section, Government Museum, Egmore, Chennai-600008,Tamilnadu, IN
Source
Indian Journal of Science and Technology, Vol 3, No 8 (2010), Pagination: 858-862Abstract
We report the spectroscopic investigation of ancient potteries excavated in Tamilnadu. Qualitative analyses were carried out to determine the major and minor constituent minerals present in the samples based on the band position or location of IR absorption peaks. From the prominent i.r. absorption peaks, the minerals were identified from the available literature. The constituents of minerals present in the potteries are further confirmed by XRD technique. Both FT-IR and XRD techniques reveals the mineral composition of ancient potteries. Energy dispersive X-ray fluorescence (XRF) was used to determine the major, minor and trace element composition of potsherds of ancient potteries. The concentration of trace elements is helpful for the characterization of pottery produced in a given region. The combined techniques are very much useful for the characterization of potteries.Keywords
Ancient Pottery, Mineral Analysis, FT-IR, XRD, EDXRF, Elemental AnalysisFull Text
References
- Benedetto GED, Laviano R, Sabbatini L and Zambonin PG (2002) Infrared spectroscopy in the mineralogical characterization of ancient pottery. J.Cul.Her. 3, 177–186.
- Chester R and Elderfield H (1967) The application of infrared absorption spectroscopy to carbonate mineralogy. Sedimentology.9, 5- 21.
- Chester R and Green RN (1968) The infrared determination of quartz in sediments and sedimentary rocks. Chem.Geo, 3, 199 -212.
- Clarence Karr. Jr (1974) Infrared and Raman Spectroscopy of lunar and terrestrial minerals. Academic Press, NY. pp: 325 -358.
- Clark RN, King TVV, Kiejwa M, Swayze, G.A. and Verge, N (1990) High spectral resolution reflectance spectra of minerals, J.Geophys Res. 95, 12653-12657.
- Coates JP (1977) The IR analysis of quartz and asbestos. Nelioth Offset Ltd., Chesham, England.
- Crowley JK and Vergo N (1988) Near- infrared reflectance of mixtures of kaolin group minerals; use in clay. Clay & Clay Minerals. 36, 310-316.
- Farmer VC (1974) The IR spectra of minerals. Mineralogical Soc., London, 42, 308-320.
- Farmer VC (1979) Infrared spectroscopy. Data hand book for clay materials and other non-metallic minerals. Ed.Van Olphen & Fripait, I Ed., Pergaman Press, Oxford, London. pp: 285 -337.
- Ghosh SN (1978) Infrared spectra of some selected minerals, rocks and products. J.Mat.Sci. 13, 1877-1886.
- Hlavay J, Jonas K, Elek S and Inczedy J (1978) Characterization of the particle size and the crystallinity of certain minerals by infrared spectrophotometry and other instrumental methods-II. Investigation on quartz and feldspar. Clay and Clay Minerals. 26, 139- 143.
- Ko TH and Chu H (2005) Spectroscopic study on sorption of hydrogen sulfide by mean of red soil. Spectro Chimica Acta. Part- A, 61, 2253–2259.
- Lyon RJP (1967) Infrared absorption spectroscopy. In: Physical methods in determinative mineralogy. Zussman J (Ed.), Academic Press, NY. pp:371-403.
- Madejova and Komadel (2001) Baseline studies of the clay minerals society source clays: Infrared methods. Clay & Clay Minerals. 49, 410-432.
- Neog AK, Boruah RK, Sahu OP, Borah PC, Ahmed W and Boruah GD (1999) XRD and IR of Deopani clay. Asian.Chem.Letts. 3,172-175.
- Ravisankar R (2009) Application of spectroscopic technoqies for the identification of minerals from beach rocks of Tamilnadu, India. Exploration & Res. for Atomic Minerals. 19, 272-276.
- Ravisankar R, Rajalakshmi A and Manikandan (2006) Mineral characterization of soil samples in and around saltfield area, Kelambakkam, Tamilnadu, India. Acta Ciencia Indica. Vol.XXXII, (3), 341 – 346.
- Reig FB, Adelankndo JVG and Moreno MCM (2002) FTIR Quantitative analysis of Calcium Carbonate (Calcite) and Silica (Quartz) mixtures using the constant ratio method; Application to geological samples. Talanta. 58, 811-815.
- Russell JD (1987) Infrared methods. In: A hand book of determinative methods in clay mineralogy, Wilson MJ (Ed.) Blackie & Son Ltd, NY, pp: 11-67
- SenthilKumar P, Parthasarathy G, Sharma DS, Srinivasan R and Krishnamurthy P (2001) Mineralogical and geochemical study on carbonate veins of Salem- Attur fault zone, Southern India: Evidence for Carbonate affinity. J.Geo.Soc.Ind. 58, 15-20.
- Sevim Akyuz, Tami Akyuz, Sait Basaran and Ahmet Gulec (2008) Analysis of ancient potteries using FT-IR, micro-Raman and EDXRF spectrometry. Viberational Spectrocopy. 48, 276-280.
- Summer ME (1995) Hand book of soil science. Univ. of Georgia, Boca Raton Hondor Press, NY.
- White JL (1971) Interpretation of infrared spectra of soil minerals. Soil science, 112, 22-67.
- Xu Z, Cornilsen BC, Popko DC, Penning WD, Wood JR and Hwang JY (2001) Quantitative mineral analysis by FT-IR spectroscopy. Int.J.Vib.Spec. 5, 4-6.