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Hydrophobic Coatings Composed by Cubic-Shaped CdO Nanoparticles Grown by a Novel and Simple Microwave Method


Affiliations
1 Institute of Material Engineering, Islamic Azad University of Najafabad, Najafabad, Isfahan 85141-43131, Iran, Islamic Republic of
2 Division of Graduate Studies and Research, Instituto Tecnologico de Toluca, Avenida Tecnologico, s/n, Colonia Agrıcola Buenavista, 52149 Metepec, MEX, Mexico
3 Apartado Postal 20, 52176 Metepec 3, MEX, Mexico
 

Cube-shaped cadmium oxide (CdO) nanoparticles were deposited by a novel low cost microwave evaporation technique. High purity cadmium(Cd) flakes were placed in a microwave susceptor inside a commercial microwave oven. Metallic Cd was evaporated in less than 2 minutes and it was oxidized due to ambient oxygen. The CdO nanoparticles were deposited on a glass substrate placed few centimeters above the susceptor. The surfaces with nanoparticles were treated with a solution containing ethanol and phenyltriethoxysilane (PTES), and the hydrophobic properties of the as-synthesized and post-PTES-treated surfaces were studied. Morphological and structural information of the as-synthesized nanoparticles were investigated via SEM and XRD analysis. Contact angles (θc) for the as-synthesized CdO surfaces were about 112, whereas, for ethanol/PTES-treated CdO nanoparticles surfaces, contact angles were improved to about 158. Thus, ethanol/PTES-treated CdO nanoparticles obtained by this simple procedure showed superhydrophobicity properties of potential use in micro fluidic devices and some other applications in the future.
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  • Hydrophobic Coatings Composed by Cubic-Shaped CdO Nanoparticles Grown by a Novel and Simple Microwave Method

Abstract Views: 78  |  PDF Views: 1

Authors

Mehrdad Rashidzadeh
Institute of Material Engineering, Islamic Azad University of Najafabad, Najafabad, Isfahan 85141-43131, Iran, Islamic Republic of
Guillermo Carbajal-Franco
Division of Graduate Studies and Research, Instituto Tecnologico de Toluca, Avenida Tecnologico, s/n, Colonia Agrıcola Buenavista, 52149 Metepec, MEX, Mexico
Arturo Tiburcio-Silver
Apartado Postal 20, 52176 Metepec 3, MEX, Mexico

Abstract


Cube-shaped cadmium oxide (CdO) nanoparticles were deposited by a novel low cost microwave evaporation technique. High purity cadmium(Cd) flakes were placed in a microwave susceptor inside a commercial microwave oven. Metallic Cd was evaporated in less than 2 minutes and it was oxidized due to ambient oxygen. The CdO nanoparticles were deposited on a glass substrate placed few centimeters above the susceptor. The surfaces with nanoparticles were treated with a solution containing ethanol and phenyltriethoxysilane (PTES), and the hydrophobic properties of the as-synthesized and post-PTES-treated surfaces were studied. Morphological and structural information of the as-synthesized nanoparticles were investigated via SEM and XRD analysis. Contact angles (θc) for the as-synthesized CdO surfaces were about 112, whereas, for ethanol/PTES-treated CdO nanoparticles surfaces, contact angles were improved to about 158. Thus, ethanol/PTES-treated CdO nanoparticles obtained by this simple procedure showed superhydrophobicity properties of potential use in micro fluidic devices and some other applications in the future.